Determination of Lead, Iron, Manganese and Zinc in Sea Water Samples by Atomic Absorption Spectrometry after Preconcentration with Chromosorb 105
Hüseyin Bağ 1  
,  
Aydan Elçi 2
,  
 
 
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1
Pamukkale University, Faculty of Education, Department of Science Education 20020, Denizli, Turkey
2
Ege University, Faculty of Science, Department of Chemistry, 35100, Bornova, İzmir, Turkey
3
Pamukkale University, Faculty of Science and Arts, Department of Chemistry, 20017, Denizli, Turkey
CORRESPONDING AUTHOR
Hüseyin Bağ   

Pamukkale University, Faculty of Education, Department of Science Education 20020, Denizli, Turkey Phone: +90‐258‐212 55 55 Fax: +90‐258‐212 78 98
Online publish date: 2006-06-01
Publish date: 2006-06-01
 
Eurasian J Anal Chem 2006;1(1):42–54
KEYWORDS
ABSTRACT
A solid phase extraction procedure based a column technique for preconcentration of lead, iron, manganese and zinc from water samples was developed. The analyte ions as its diethyldithiocarbamate complex were retained on a column of Chromosorb 105 from buffered sample solution. Then they were eluted with acetone. The recoveries of lead, iron, manganese and zinc under the optimum working conditions were 100, 97, 100 and 100%, respectively. The relative standard deviations were less than 6%. The method presented was applied for the determination of lead, iron, zinc and manganese in sea water samples.
 
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